https://dlj.law.duke.edu/article/patent-laws-reproducibility...
What you're talking about is called a 112 rejection. Section 112 has to do with "written description," "enablement," and "best mode."
Getting a patent invalidated after it's issued can't be done on 112 grounds. It's done based on anticipation and obviousness (prior art, basically).
The legal fiction is that a "reasonable amount of experimentation" may be required, beyond what's in the patent. The notion is that a lab tech determines the exact concentrations, temps, and pressure to get the thing to work.
Of course this is abused.
He could have argued they maybe should have originally been covered by https://www.wikipedia.org/wiki/Invention_Secrecy_Act to begin with maybe.
e.g. "How Turkey Defied the U.S. and Became a Killer Drone Power" https://theintercept.com/2019/05/14/turkey-second-drone-age/
That's why important stuff is kept secret.